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If using a vial, wipe the rubber stopper with an alcohol swab, insert the needle, invert the vial, and draw the prescribed volume (typically 0.5 to 1 mL)

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If you want to calculate a corrosion rate for them anyway, you need to measure in which mole fraction the alloy dissolves, for example by investigating the solution in contact with the alloy before and after a corrosion event